反应条件
1: 78 percent / KF / 18-crown-6 / tetrahydrofuran / 1 h / 2 °C
2: 28percent aq. NH4OH / aq. ethanol / 0.5 h / 25 °C
3: CSA / CH2Cl2 / 1 h / 25 °C
4: n-Bu3SnH, AIBN / toluene / 0.33 h / 110 °C
5: 10percent aq. AcOH / acetone / 14 h / 25 °C
6: 5percent NaOMe / methanol / 2 h / 25 °C
7: Na / liquid ammonia / 0.5 h / -78 °C
View Scheme
参考文献
Yoshikawa; Okaichi; Cha; Kitagawa
Tetrahedron, 1990 , vol. 46, # 21 p. 7459 - 7470
