2,6-二氯-3-甲氧基吡啶合成路线 （共 2 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
MERCK SHARP and DOHME CORP.; MCCOMAS, Casey Cameron; LIVERTON, Nigel J.; HABERMANN, Joerg; KOCH, Uwe; NARJES, Frank; LI, Peng; PENG, Xuanjia; SOLL, Richard; WU, Hao; PALANI, Anandan; HE, Shuwen; DAI, Xing; LIU, Hong; LAI, Zhong; LONDON, Clare; XIAO, Dong; ZORN, Nicolas; NARGUND, Ravi
Patent: WO2013/33971 A1, 2013 ;
Location in patent: Page/Page column 33 ;
反应条件
1: dihydrogen peroxide / dichloromethane; water / 0.15 h / 0 - 20 °C 2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C View Scheme
参考文献
MERCK SHARP and DOHME CORP.; MCCOMAS, Casey Cameron; LIVERTON, Nigel J.; HABERMANN, Joerg; KOCH, Uwe; NARJES, Frank; LI, Peng; PENG, Xuanjia; SOLL, Richard; WU, Hao; PALANI, Anandan; HE, Shuwen; DAI, Xing; LIU, Hong; LAI, Zhong; LONDON, Clare; XIAO, Dong; ZORN, Nicolas; NARGUND, Ravi
Patent: WO2013/33971 A1, 2013 ;
