(1-硝基-2-苯乙烯基)苯合成路线 （共 17 条）
反应条件
1: 71 percent / DBU / tetrahydrofuran / 12 h / Ambient temperature
2: 85 percent / NaOH / ethane-1,2-diol / 2 h / 170 °C
View Scheme
参考文献
Ono, Noboru; Miyagawa, Hirokazu; Ueta, Takahiro; Ogawa, Takuji; Tani, Hiroyuki
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 10 p. 1595 - 1601
反应条件
1: tetrahydrofuran / -78 °C
2: 94 percent / hydrogen / Pd(OH)2/C / ethanol / 70 °C / 750.08 Torr
View Scheme
参考文献
Fessard, Thomas C.; Motoyoshi, Hajime; Carreira, Erick M.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 12 p. 2078 - 2081
反应条件
sodium hypochlorite; triethylamine in dichloromethane
T=20°C; 24 h;
参考文献
Ganesh, Madhu; Namboothiri, Irishi N.N.
Tetrahedron, 2007 , vol. 63, # 48 p. 11973 - 11983
反应条件
bei der Destillation im Vakuum;
参考文献
Heim
Chemische Berichte, 1911 , vol. 44, p. 2017
参考文献
Gruenanger
Gazzetta Chimica Italiana, 1954 , vol. 84, p. 359,367
反应条件
potassium fluoride; potassium fluorosulfite
参考文献
Hoz,S. et al.
Synthesis, 1975 , p. 162
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran; isopropyl alcohol / 0 - 20 °C / Inert atmosphere
2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
3: dihydrogen peroxide; sodium hydrogencarbonate / methanol / 20 °C / Inert atmosphere
View Scheme
参考文献
Greger, Jessica G.; Yoon-Miller, Sarah J. P.; Bechtold, Nathan R.; Flewelling, Scott A.; MacDonald, Jacob P.; Downey, Catherine R.; Cohen, Eric A.; Pelkey, Erin T.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8203 - 8214
