9-羟基-9-芴甲酸甲酯合成路线 （共 11 条）
反应条件
sulfuric acid 1 h; Heating / reflux;
参考文献
Boehringer Ingelheim Pharma GmbH. Co. KG
Patent: US2003/207912 A1, 2003 ;
Location in patent: Page 9 ;
反应条件
in benzene T=110°C; 20 h;
参考文献
Journal of Organic Chemistry, , vol. 62, # 12 p. 4065 - 4067
反应条件
oxygen; lithium diisopropyl amide 1.) THF, hexane, -32 deg C, 2.) THF, hexane, RT, 8.5 h; Yield given. Multistep reaction;
参考文献
Journal of Heterocyclic Chemistry, , vol. 32, # 3 p. 1051 - 1056
反应条件
1: 1.) lithium dicyclohexylamide / 2) THF, -78 deg C, 2 h 2: Hg(ClO4)2*3H2O / 0.42 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 11, # 3 p. 209 - 216
反应条件
mercury(II) perchlorate 0.416667 h; Ambient temperature; Yield given;
参考文献
Synthetic Communications, , vol. 11, # 3 p. 209 - 216
反应条件
oxygen; lithium diisopropyl amide 1.) THF, hexane, -32 deg C, 2.) THF, hexane, -32 deg C, 6 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Heterocyclic Chemistry, , vol. 32, # 3 p. 1051 - 1056
反应条件
1: aq. barium hydroxide solution 2: hydrogen chloride View Scheme
参考文献
Chemische Berichte, , vol. 39, p. 3065
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>133, p. 313
参考文献
Lew; Wagner; Angelini, Mark P.; Lee-Ruff; Lusztyk; Johnston
Journal of the American Chemical Society, 1996 , vol. 118, # 48 p. 12066 - 12073
