反应条件
Multi-step reaction with 3 steps 1: 61 percent / DIBAL / toluene / 12 h / Ambient temperature2: SmI2, t-BuOH / tetrahydrofuran / 0.17 h3: 1.) methyl(diphenyl)phosphine, 2.) MCPBA / 1.) MeCN, room temperature, 12 h, 2.) CH2Cl2, ca. 0 deg C, 3 h
参考文献
Arai, Yoshitsugu; Hayashi, Kazuya; Matsui, Makoto; Koizumi, Toru; Shiro, Motoo; Kuriyama, Kaoru Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 7 p. 1709 - 1716
