4’-羟基联苯-3-羧酸合成路线 (共 10 条)
反应条件
1: With dipotassium peroxodisulfate; trifluoroacetic acid; palladium (II) trifluoroacetate in dichloromethane T=50°C; 48 h; 2: With water in dichloromethane
参考文献
Organic Letters, , vol. 6, # 14 p. 2437 - 2439
反应条件
1: With dipotassium peroxodisulfate; trifluoroacetic acid; palladium (II) trifluoroacetate in dichloromethane T=50°C; 48 h; 2: With water in dichloromethane
参考文献
Organic Letters, , vol. 6, # 14 p. 2437 - 2439
反应条件
{C6H3[NHP(piperidinyl)2]2Pd(Cl)}; potassium carbonate in 1,4-dioxane; water; butan-1-ol T=100°C; Suzuki-Miyaura reaction; 6 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 352, # 6 p. 1075 - 1080
反应条件
dipotassium peroxodisulfate; trifluoroacetic acid; palladium (II) trifluoroacetate in dichloromethane T=50°C; 48 h;
参考文献
Organic Letters, , vol. 6, # 14 p. 2437 - 2439
反应条件
ethylenediaminetetraacetic acid; potassium carbonate; palladium dichloride T=100°C; Suzuki-Miyaura reaction; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 46, # 34 p. 5751 - 5754
反应条件
hydrogen bromide; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 75, p. 4969,4972
反应条件
1: KMnO4 2: aqueous HBr; acetic acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 75, p. 4969,4972
反应条件
1: diethyl ether / Erhitzen des Reaktionsprodukts mit Essigsaeure, Acetanhydrid und Naphthalin-2-sulfonsaeure und anschliessend mit Schwefel 2: KMnO4 3: aqueous HBr; acetic acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 75, p. 4969,4972
反应条件
1: diethyl ether / Erhitzen des Reaktionsprodukts mit Essigsaeure, Acetanhydrid und Naphthalin-2-sulfonsaeure und anschliessend mit Schwefel 2: KMnO4 3: aqueous HBr; acetic acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 75, p. 4969,4972
反应条件
anhydrous sodium hydrogen carbonate; sulfuric acid in methanol
参考文献
Astra Pharmaeuticals Ltd.
Patent: US5977105 A1, 1999 ;
US 5977105 A