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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
121702-30-5
合成路线
（共 9 条）
121702-30-5
→
反应条件
37464-90-7
5,8-二甲氧基-3,4-二氢-1H-2-萘酮
反应条件
1: 83 percent / LAH / tetrahydrofuran / 4 h / Ambient temperature 2: pyridinium dichromate / or PCC View Scheme
参考文献
Mehendale, A. R.; Kulkarni, Alpana; Nagarajan, Geeta
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. <B> 27, # 1-12 p. 305 - 307
121702-30-5
→
反应条件
65529-77-3
反应条件
1: 83 percent / LAH / tetrahydrofuran / 4 h / Ambient temperature 2: 69 percent / p-toluenesulphonic acid / acetonitrile / 0.5 h / 0 deg C to room temperature 3: 86 percent / aluminium chloride, LAH / diethyl ether / 1 h / 5 °C 4: 67.1 percent / pyridinium dichromate / CH2Cl2; acetic anhydride / 2 h / Heating 5: 85 percent / diethyl ether / 1 h / Ambient temperature 6: 71 percent / pyridinium dichromate / CH2Cl2; acetic anhydride / 2 h / Heating 7: 75 percent / aluminium chloride, sodium chloride / 0.08 h / 180 - 190 °C View Scheme
参考文献
Mehendale, A. R.; Kulkarni, Alpana; Nagarajan, Geeta
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. <B> 27, # 1-12 p. 305 - 307
121702-30-5
→
反应条件
121637-70-5
反应条件
With lithium aluminium tetrahydride in tetrahydrofuran 4 h; Ambient temperature;
参考文献
Mehendale, A. R.; Kulkarni, Alpana; Nagarajan, Geeta Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. <B> 27, # 1-12 p. 305 - 307
121702-30-5
→
反应条件
121637-71-6
反应条件
Multi-step reaction with 2 steps 1: 83 percent / LAH / tetrahydrofuran / 4 h / Ambient temperature2: 69 percent / p-toluenesulphonic acid / acetonitrile / 0.5 h / 0 deg C to room temperature
参考文献
Mehendale, A. R.; Kulkarni, Alpana; Nagarajan, Geeta Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. <B> 27, # 1-12 p. 305 - 307
121702-30-5
→
反应条件
121637-72-7
反应条件
Multi-step reaction with 3 steps 1: 83 percent / LAH / tetrahydrofuran / 4 h / Ambient temperature2: 69 percent / p-toluenesulphonic acid / acetonitrile / 0.5 h / 0 deg C to room temperature3: 86 percent / aluminium chloride, LAH / diethyl ether / 1 h / 5 °C
参考文献
Mehendale, A. R.; Kulkarni, Alpana; Nagarajan, Geeta Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. <B> 27, # 1-12 p. 305 - 307
121702-30-5
→
反应条件
121637-73-8
反应条件
Multi-step reaction with 4 steps 1: 83 percent / LAH / tetrahydrofuran / 4 h / Ambient temperature2: 69 percent / p-toluenesulphonic acid / acetonitrile / 0.5 h / 0 deg C to room temperature3: 86 percent / aluminium chloride, LAH / diethyl ether / 1 h / 5 °C4: 67.1 percent / pyridinium dichromate / CH2Cl2; acetic anhydride / 2 h / Heating
参考文献
Mehendale, A. R.; Kulkarni, Alpana; Nagarajan, Geeta Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. <B> 27, # 1-12 p. 305 - 307
121702-30-5
→
反应条件
121637-74-9
反应条件
Multi-step reaction with 5 steps 1: 83 percent / LAH / tetrahydrofuran / 4 h / Ambient temperature2: 69 percent / p-toluenesulphonic acid / acetonitrile / 0.5 h / 0 deg C to room temperature3: 86 percent / aluminium chloride, LAH / diethyl ether / 1 h / 5 °C4: 67.1 percent / pyridinium dichromate / CH2Cl2; acetic anhydride / 2 h / Heating5: 85 percent / diethyl ether / 1 h / Ambient temperature
参考文献
Mehendale, A. R.; Kulkarni, Alpana; Nagarajan, Geeta Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. <B> 27, # 1-12 p. 305 - 307
121702-30-5
→
反应条件
121637-75-0
反应条件
Multi-step reaction with 6 steps 1: 83 percent / LAH / tetrahydrofuran / 4 h / Ambient temperature2: 69 percent / p-toluenesulphonic acid / acetonitrile / 0.5 h / 0 deg C to room temperature3: 86 percent / aluminium chloride, LAH / diethyl ether / 1 h / 5 °C4: 67.1 percent / pyridinium dichromate / CH2Cl2; acetic anhydride / 2 h / Heating5: 85 percent / diethyl ether / 1 h / Ambient temperature6: 71 percent / pyridinium dichromate / CH2Cl2; acetic anhydride / 2 h / Heating
参考文献
Mehendale, A. R.; Kulkarni, Alpana; Nagarajan, Geeta Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. <B> 27, # 1-12 p. 305 - 307
112997-44-1
→
反应条件
121702-30-5
反应条件
With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium 4 h; Ambient temperature;
参考文献
Mehendale, A. R.; Kulkarni, Alpana; Nagarajan, Geeta Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. <B> 27, # 1-12 p. 305 - 307
