2,7-二氯-3,6-双[[(1,1-二甲基乙基)二甲基硅]氧基]-9H-氧杂蒽-9-酮合成路线 （共 4 条）
反应条件
1H-imidazole in N,N-dimethyl-formamide T=20°C;
参考文献
Kenmoku, Suguru; Urano, Yasuteru; Kanda, Koujirou; Kojima, Hirotatsu; Kikuchi, Kazuya; Nagano, Tetuso
Tetrahedron, 2004 , vol. 60, # 49 p. 11067 - 11073
参考文献
Nagano, Tetsuo; Daiichi Pure Chemicals Co., Ltd.
Patent: US7524974 B2, 2009 ;
Location in patent: Page/Page column 18-19 ;
反应条件
1: 17 percent / POCl3; ZnCl2 / 12 h / 20 °C 2: 100 percent / H2O / 220 °C / 1900 Torr 3: 53 percent / imidazole / dimethylformamide / 20 °C View Scheme
参考文献
Kenmoku, Suguru; Urano, Yasuteru; Kanda, Koujirou; Kojima, Hirotatsu; Kikuchi, Kazuya; Nagano, Tetuso
Tetrahedron, 2004 , vol. 60, # 49 p. 11067 - 11073
反应条件
1: 17 percent / POCl3; ZnCl2 / 12 h / 20 °C 2: 100 percent / H2O / 220 °C / 1900 Torr 3: 53 percent / imidazole / dimethylformamide / 20 °C View Scheme
参考文献
Kenmoku, Suguru; Urano, Yasuteru; Kanda, Koujirou; Kojima, Hirotatsu; Kikuchi, Kazuya; Nagano, Tetuso
Tetrahedron, 2004 , vol. 60, # 49 p. 11067 - 11073
