反应条件
in dichloromethane
N2; treatment of Ph3CPF6 with Cp(CO)3MoH (-78°C, then -20°C, 10 min), addn. of Fe-complex (molar ratio Mo:Ph3CPF6:Fe = 2:2:1), warming to room temp., stirring (room temp., 1 h); pptn., filtration, washing (CH2Cl2), drying; contains traces of (Cp(CO)3Mo)2;
参考文献
Markham, James; Tolman, William; Menard, Kevin; Cutler, Alan
Journal of Organometallic Chemistry, 1985 , vol. 294, p. 45 - 58
