3-(2-呋喃基)-L-丙氨酸合成路线 (共 15 条)
反应条件
1: 1,4-dioxane / 24 h / Reflux 2: potassium hydroxide / 17 h / 20 °C 3: porcine kidney acylase 1; cobalt(II) chloride / Enzymatic reaction View Scheme
参考文献
ChemBioChem, , vol. 11, # 12 p. 1720 - 1726
反应条件
1: 90 percent / aq. KOH / 4 h / Heating 2: 66 percent / phenylalanine ammonia-lyase; aq. NH3; CO2 / 72 h / 30 °C / pH 10.2 View Scheme
参考文献
Chemistry - A European Journal, , vol. 12, # 10 p. 2739 - 2744
反应条件
1: potassium hydroxide / 17 h / 20 °C 2: porcine kidney acylase 1; cobalt(II) chloride / Enzymatic reaction View Scheme
参考文献
ChemBioChem, , vol. 11, # 12 p. 1720 - 1726
反应条件
triethylamine in methanol T=60°C; 0.5 h;
参考文献
Berthel, Steven Joseph; Brinkman, John A.; Hayden, Stuart; Haynes, Nancy-Ellen; Kester, Robert Francis; McDermott, Lee Apostle; Qian, Yimin; Sarabu, Ramakanth; Scott, Nathan Robert; Tilley, Jefferson Wright
Patent: US2009/264445 A1, 2009 ;
Location in patent: Page/Page column 38 ;
反应条件
alanine racemase (accession number AE015451 range 4,245,041-4,246,270), cloned from the genome of Pseudomonas putida (KT2440) in water; glycerol
T=31°C; 1 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Cox, Brad M.; Bilsborrow, Joshua B.; Walker, Kevin D.
Journal of Organic Chemistry, 2009 , vol. 74, # 18 p. 6953 - 6959