10,10’-二溴-9,9’-联二蒽合成路线 （共 12 条）
反应条件
Cu(OH)x has been encapsulated over montmorillonite-KSF; air in methanol T=20°C; 1 h; Green chemistry;
参考文献
Dar, Bashir Ahmad; Singh, Snehil; Pandey, Nalini; Singh; Sharma, Priti; Lazar, Anish; Sharma, Meena; Vishwakarma, Ram A.; Singh, Baldev
Applied Catalysis A: General, 2014 , vol. 470, p. 232 - 238
反应条件
bromine in carbon disulfide 30 h; Ambient temperature;
参考文献
Baumgarten, Martin; Yueksel, Timucin
Physical Chemistry Chemical Physics, 1999 , vol. 1, # 8 p. 1699 - 1706
反应条件
triphenyl phosphite; palladium diacetate; caesium carbonate in N,N-dimethyl-formamide T=75°C;
参考文献
Tetrahedron Letters, , vol. 51, # 19 p. 2655 - 2656
反应条件
triphenyl phosphite; sodium acetate; palladium diacetate in N,N-dimethyl-formamide T=75°C;
参考文献
Tetrahedron Letters, , vol. 51, # 19 p. 2655 - 2656
反应条件
bromine in various solvent(s) Ambient temperature;
参考文献
Herges, Rainer; Neumann, Helfried
Liebigs Annalen, 1995 , # 7 p. 1283 - 1290
反应条件
1: zinc; zinc(II) chloride; water / tetrahydrofuran / 36 h / 20 °C / |Inert atmosphere 2: toluene-4-sulfonic acid / toluene / 2 h / |Inert atmosphere; |Reflux 3: bromine / tetrachloromethane / 4 h / 0 - 20 °C / |Cooling with ice View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 20 p. 10383 - 10394
反应条件
1: toluene-4-sulfonic acid / toluene / 2 h / |Inert atmosphere; |Reflux 2: bromine / tetrachloromethane / 4 h / 0 - 20 °C / |Cooling with ice View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 20 p. 10383 - 10394
反应条件
1: zinc; hydrogenchloride; acetic acid 2: bromine / 1,2-dichloro-ethane View Scheme
参考文献
Journal of Materials Chemistry C, , vol. 1, # 48 p. 8117 - 8127
反应条件
bromine Title compound not separated from byproducts;
参考文献
Liebigs Annalen, , # 7 p. 1283 - 1290
反应条件
in benzene Irradiationphotolysis; also in 1,4-dioxane, acetonitrile; Product distribution;
参考文献
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, , vol. 36, # 7 p. 846 - 851
