10,10’-二溴-9,9’-联二蒽合成路线 (共 12 条)
反应条件
n-butyllithium; iodine 1.) Et2O, hexane, room temperature, 15 min, 2.) Et2O, 2 h; Yield givenMultistep reaction;
参考文献
Baumgarten, Martin; Yueksel, Timucin
Physical Chemistry Chemical Physics, 1999 , vol. 1, # 8 p. 1699 - 1706
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in water; toluene Suzuki cross-coupling reaction; 4 h; Reflux;
参考文献
Jang, Heung Soo; Lee, Kum Hee; Lee, Seok Jae; Kim, Young Kwan; Yoon, Seung Soo
Molecular Crystals and Liquid Crystals, 2012 , vol. 563, p. 173 - 184