Deshmukh, G. S.; Kane, Y. D.
Proc. Indian Acad. Sci., 1947 , vol. 25 A, p. 247 - 255
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Gmelin Handbook: P: MVol.B, 3.4.2.1, page 306 - 307
in carbon disulfide under N2, dropwise addn. of a Br2/CS2 soln. to a vigorously stirred soln. of P4/CS2 reaction of P4 with ICl (molar ratio (1.75:1.5), further Products: ClIP2ClI, ClIP2I2, P2I4, P7I3; not isolated, identified by 31P-NMR spectroscopy;
参考文献
Tattershall, Bruce W.; Kendall, Nigel L.
Polyhedron, 1994 , vol. 13, p. 1517 - 1522
trimethylstannyl chloride in carbon disulfide reaction of P4 with Br2 in CS2, followed by treatment with C(CH3)3SnCl; further products: Cl2P2Br2, ClBrP2ClBr, P2Br4, PBr3; not isolated, identified by 31P-NMR spectroscopy;
参考文献
Tattershall, Bruce W.; Kendall, Nigel L.
Polyhedron, 1994 , vol. 13, p. 1517 - 1522
sodium hydroxyde in water; water-d2 heating under 150 Torr N2 gas with a luminous flame until the phosphorus melted, phosphine was condensed at liquid nitrogen temp.;
参考文献
McRae, Glenn A.; Gerry, M. C. L.; Cohen, E. A.
Journal of Molecular Spectroscopy, 1986 , vol. 116, p. 58 - 70
sodium hydroxyde in water; water-d2 heating under 150 Torr N2 gas with a luminous flame until the phosphorus melted, phosphine was condensed at liquid nitrogen temp.;
参考文献
McRae, Glenn A.; Gerry, M. C. L.; Cohen, E. A.
Journal of Molecular Spectroscopy, 1986 , vol. 116, p. 58 - 70
