1,3-双(4-氯苯基)尿素合成路线 (共 117 条)
反应条件
[bis(acetoxy)iodo]benzene; water in dichloromethane
T=20 - 40°C; Hofmann rearrangement; 17 h;
参考文献
Landsberg, Dirk; Kalesse, Markus
Synlett, 2010 , # 7 p. 1104 - 1106
反应条件
4-(N,N-dimethlyamino)pyridine; W(CO)6; iodine in dichloromethane
T=40°C; P=60804.1 Torr; 20 h;
参考文献
Zhang, Li; Darko, Ampofo K.; Johns, Jennifer I.; McElwee-White, Lisa
European Journal of Organic Chemistry, 2011 , # 31 p. 6261 - 6268
参考文献
Beaver et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 1236,1242
Journal of Organic Chemistry, 1959 , vol. 24, p. 1676
反应条件
dichlorotris(triphenylphosphine)ruthenium(II) in 1,3,5-trimethyl-benzene
12 h; Heating;
参考文献
Kotachi, Shinji; Tsuji, Yasushi; Kondo, Teruyuki; Watanabe, Yoshihisa
Journal of the Chemical Society, Chemical Communications, 1990 , # 7 p. 549 - 550
反应条件
carbon monoxide; benzene; dodecacarbonyltetrarhodium(0)
T=220°C; 6 h;
参考文献
Mise, Takaya; Hong, Pangbu; Yamazaki, Hiroshi
Chemistry Letters, 1980 , p. 439 - 440
反应条件
1,2,4,5-tetramethyl benzene; caesium carbonate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in 1,4-dioxane
T=100°C; 10 h;
参考文献
Sergeev; Artamkina; Beletskaya
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 12 p. 1741 - 1752
反应条件
4-(N,N-dimethlyamino)pyridine; W(CO)6; iodine in dichloromethane
T=40°C; P=60804.1 Torr; 20 h;
参考文献
Zhang, Li; Darko, Ampofo K.; Johns, Jennifer I.; McElwee-White, Lisa
European Journal of Organic Chemistry, 2011 , # 31 p. 6261 - 6268
反应条件
copper acetylacetonate; potassium tert-butylate in 1-methyl-pyrrolidin-2-one
T=20°C; 24 h; Inert atmosphereSealed vial;
参考文献
Gavade, Sandip; Balaskar, Ravi; Mane, Madhav; Pabrekar, Pramod N.; Mane, Dhananjay
Synthetic Communications, 2012 , vol. 42, # 11 p. 1704 - 1714
反应条件
TEA in benzene
Heating;
参考文献
Mataka, Shuntaro; Irie, Takashi; Ikezaki, Youji; Tashiro, Masashi
Chemische Berichte, 1993 , vol. 126, # 8 p. 1819 - 1822
反应条件
benzene; dodecacarbonyltetrarhodium(0)
T=220°C; 6 h;
参考文献
Mise, Takaya; Hong, Pangbu; Yamazaki, Hiroshi
Chemistry Letters, 1980 , p. 439 - 440