1,3-双(4-氯苯基)尿素合成路线 (共 117 条)
反应条件
di-tert-butyl peroxide in chlorobenzene
T=110°C; 48 h; Further byproducts given;
参考文献
Leardini, Rino; Tundo, Antonio; Zanardi, Giuseppe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3164 - 3167
反应条件
di-tert-butyl peroxide in chlorobenzene
T=110°C; 48 h; Further byproducts given;
参考文献
Leardini, Rino; Tundo, Antonio; Zanardi, Giuseppe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3164 - 3167
反应条件
1,10-phenanthroline; Pd(1,10-phenanthroline)2(OTf)2
T=135°C; P=45003.6 Torr; 2 h; Yield given. Further byproducts given;
参考文献
Wchman, Petra; Borst, Leo; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
Chemische Berichte, 1997 , vol. 130, # 1 p. 13 - 21
反应条件
zeolite HSZ-360
T=180°C; 5 h; Yield given;
参考文献
Bigi, Franca; Maggi, Raimondo; Sartori, Giovanni; Zambonin, Elena
Chemical Communications, 1998 , # 4 p. 513 - 514
反应条件
1: acetic acid
View Scheme
参考文献
Young; Dunstan
Journal of the Chemical Society, 1908 , vol. 93, p. 1055,1057
反应条件
sodium hydroxide in acetonitrile
参考文献
Stevens,T.E.
Journal of Organic Chemistry, 1961 , vol. 26, p. 3451 - 3457
反应条件
isoarecolinol in diethyl ether
24 h; Ambient temperature;
参考文献
Lambrecht, Guenter; Moser, Ulrich; Mutschler, Ernst; Walther, Gerhard; Wess, Juergen
Journal of Medicinal Chemistry, 1986 , vol. 29, # 7 p. 1309 - 1311
反应条件
sodium hydride in tetrahydrofuran
288 h; Ambient temperature;
参考文献
Budny, Jochen; Stamm, Helmut
Archiv der Pharmazie (Weinheim, Germany), 1981 , vol. 314, # 8 p. 657 - 664
反应条件
triethylamine in diethyl ether
Heating;
参考文献
Shimizu, Tomio; Hayashi, Yoshiyuki; Teramura, Kazuhiro
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 2038 - 2040
反应条件
ethanol
0.0166667 h; Microwave irradiationNeat (no solvent);
参考文献
Uberhande; Thakare; Berad
Journal of the Indian Chemical Society, 2010 , vol. 87, # 9 p. 1137 - 1141