6-甲基-2-苯基-喹唑啉合成路线 (共 13 条)
反应条件
1.1: 1-methyl-pyrrolidin-2-one / 24 h / |Reflux
2.1: borane-THF / tetrahydrofuran / |Inert atmosphere; |Reflux
3.1: chloroform / 4 h / 35 °C
3.2: polymer-supported bi-metallic platinum/iridium (Pt/Ir) alloyed nanoclusters / 16 h / 35 °C / 760.05 Torr
View Scheme
参考文献
Yuan, Hao; Yoo, Woo-Jin; Miyamura, Hiroyuki; Kobayashi, Shu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 16 p. 2899 - 2904
反应条件
1.1: iodine; sodium hydrogencarbonate / dichloromethane; water / 20 °C
2.1: 1-methyl-pyrrolidin-2-one / 24 h / |Reflux
3.1: borane-THF / tetrahydrofuran / |Inert atmosphere; |Reflux
4.1: chloroform / 4 h / 35 °C
4.2: polymer-supported bi-metallic platinum/iridium (Pt/Ir) alloyed nanoclusters / 16 h / 35 °C / 760.05 Torr
View Scheme
参考文献
Yuan, Hao; Yoo, Woo-Jin; Miyamura, Hiroyuki; Kobayashi, Shu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 16 p. 2899 - 2904
反应条件
ueber den Schmelzpunkt;
参考文献
Bischler; Muntendam
Chemische Berichte, 1895 , vol. 28, p. 729