3-(叔丁基二甲基甲硅烷基氧基)苯胺合成路线 (共 5 条)
反应条件
1H-imidazole in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Petronijevic, Filip R.; Wipf, Peter
Journal of the American Chemical Society, 2011 , vol. 133, # 20 p. 7704 - 7707
反应条件
1: Py / CH2Cl2 2: NaH / dimethylformamide 3: aq. K2CO3 / methanol 4: aq. NaNO2, HCl / tetrahydrofuran View Scheme
参考文献
Watanabe; Takeuchi; Otsuka; Tanaka; Umezawa
Journal of Antibiotics, 1995 , vol. 48, # 12 p. 1460 - 1466
反应条件
1.1: 95 percent / tetrahydrofuran 2.1: 95 percent / TBAF / CH2Cl2 3.1: NaH / dimethylformamide 3.2: dimethylformamide 4.1: SnCl4 / ethyl acetate; methanol; diethyl ether View Scheme
参考文献
Boussard, Cyrille; Klimkait, Thomas; Mahmood, Naheed; Pritchard, Martin; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 10 p. 2673 - 2676
反应条件
Na3PO4*12H2O in N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
Synthetic Communications, , vol. 42, # 2 p. 285 - 291
反应条件
1: Py / CH2Cl2 2: NaH / dimethylformamide 3: aq. K2CO3 / methanol View Scheme
参考文献
Watanabe; Takeuchi; Otsuka; Tanaka; Umezawa
Journal of Antibiotics, 1995 , vol. 48, # 12 p. 1460 - 1466