(Z)-5-氯-3-羟基-2-亚甲基-5-苯基-4-戊烯腈合成路线 (共 3 条)
反应条件
1,4-diaza-bicyclo[2.2.2]octane T=50°C; Baylis-Hillman reaction; 3.5 h; Neat (no solvent)Sonication;
参考文献
Zhong, Weihui; Jiang, Lingbo; Guo, Baoming; Wu, Yaotiao; Hong, Lingjuan; Chen, Yanhui
Synthetic Communications, 2010 , vol. 40, # 16 p. 2441 - 2456
反应条件
bis(trichloromethyl) carbonate; triethylamine; triphenyl-phosphine oxide in dichloromethane T=0 - 20°C; stereoselective reaction;
参考文献
Zhong, Weihui; Hong, Lingjuan; Zheng, Yemin
Letters in Organic Chemistry, 2010 , vol. 7, # 3 p. 229 - 234
反应条件
bromine; triphenylphosphine in dichloromethane T=0 - 20°C; stereoselective reaction;
参考文献
Zhong, Weihui; Jiang, Lingbo; Guo, Baoming; Wu, Yaotiao; Hong, Lingjuan; Chen, Yanhui
Synthetic Communications, 2010 , vol. 40, # 16 p. 2441 - 2456