4,5,9,10-四溴-2,7-二(2-辛基十二烷基)苯并[lmn][3,8]菲咯啉-1,3,6,8(2H,7H)-四酮合成路线 （共 3 条）
反应条件
propionic acid in o-xylene T=140°C; 2 h;
参考文献
Steyrleuthner, Robert; Di Pietro, Riccardo; Collins, Brian A.; Polzer, Frank; Himmelberger, Scott; Schubert, Marcel; Chen, Zhihua; Zhang, Shiming; Salleo, Alberto; Ade, Harald; Facchetti, Antonio; Neher, Dieter
Journal of the American Chemical Society, 2014 , vol. 136, # 11 p. 4245 - 4256
反应条件
1.1: sulfuric acid, fuming / 2 h / 55 °C 1.2: 50 h / 85 °C 2.1: propionic acid / o-xylene / 2 h / 140 °C View Scheme
参考文献
Steyrleuthner, Robert; Di Pietro, Riccardo; Collins, Brian A.; Polzer, Frank; Himmelberger, Scott; Schubert, Marcel; Chen, Zhihua; Zhang, Shiming; Salleo, Alberto; Ade, Harald; Facchetti, Antonio; Neher, Dieter
Journal of the American Chemical Society, 2014 , vol. 136, # 11 p. 4245 - 4256
反应条件
acetic acid; zinc in water; isopropyl alcohol T=90°C; Inert atmosphere; Overall yield = 49 percent; Overall yield = 0.71 g;
参考文献
Steyrleuthner, Robert; Di Pietro, Riccardo; Collins, Brian A.; Polzer, Frank; Himmelberger, Scott; Schubert, Marcel; Chen, Zhihua; Zhang, Shiming; Salleo, Alberto; Ade, Harald; Facchetti, Antonio; Neher, Dieter
Journal of the American Chemical Society, 2014 , vol. 136, # 11 p. 4245 - 4256
