反应条件
1: 1) (COCl)2, DMSO, 2) Et3N
2: MCPBA / CH2Cl2 / 3 h / phosphate buffer (pH 7)
3: LiAlH4 / diethyl ether / 1 h / 0 °C
4: 1) (COCl)2, DMSO, 2) Et3N
View Scheme
参考文献
Wang, Yuan; Babirad, Stefan A.; Kishi, Yoshito
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 468 - 481