反应条件
1.1: formic acid; triethylamine 1.2: Reflux 2.1: sec.-butyllithium / diethyl ether; hexane; cyclohexane / -78 - -70 °C / Inert atmosphere 2.2: -78 - -70 °C / Inert atmosphere 2.3: -78 - 20 °C 3.1: tetrabutyl ammonium fluoride; water / pentane / 12 h / 50 °C / Sealed tube 4.1: oxygen; ozone / methanol; dichloromethane / 0.25 h / -78 °C 4.2: -78 - 20 °C / Inert atmosphere View Scheme
参考文献
Aggarwal, Varinder K.; Ball, Liam T.; Carobene, Simon; Connelly, Rickki L.; Hesse, Matthew J.; Partridge, Benjamin M.; Roth, Philippe; Thomas, Stephen P.; Webster, Matthew P.
Chemical Communications, 2012 , vol. 48, # 74 p. 9230 - 9232
