1: 83 percent / pyridine / Ambient temperature
2: PCl5 / 1.5 h / 130 °C
3: sodium azide, sodium acetate / acetone; H2O / 8 h
4: 50 percent / decahydronaphthalene / 2 h / Heating
View Scheme
参考文献
Ramachandraiah, G.; Reddy, K. Kondal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 808 - 810
Liepin'sh, E. E.; Zitsmane, I. A.; Ignatovich, L. M.; Lukevits, E.; Guvanova, L. I.; Voronkov, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1789 - 1792,1609 - 1612
1: vinyl ethyl ketone With indium(III) chloride; indium in water; acetonitrile
T=20°C; 24 h;
2: 4-chloro-benzoyl chloride With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
24 h; Reflux;
参考文献
Shen, Zhi-Liang; Goh, Kelvin Kau Kiat; Cheong, Hao-Lun; Wong, Colin Hong An; Lai, Yin-Chang; Yang, Yong-Sheng; Loh, Teck-Peng
Journal of the American Chemical Society, 2010 , vol. 132, # 45 p. 15852 - 15855
