反应条件
1: hydrazine hydrate / methanol / 0.5 h / |Reflux; |Inert atmosphere 2: N,N-dimethyl acetamide / 6 h / 0 °C / |Inert atmosphere 3: trichlorophosphate / 20 h / 80 °C / |Inert atmosphere 4: Na2S*9H2O / 1,4-dioxane; water / 0.75 h / 80 °C / |Inert atmosphere View Scheme
参考文献
Conole, Daniel; Beck, Thorsten M.; Jay-Smith, Morgan; Tingle, Malcolm D.; Eason, Charles T.; Brimble, Margaret A.; Rennison, David
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 7 p. 2220 - 2235