反应条件
1: 72 percent / AlCl3 / CS2 / 1 h / Ambient temperature
2: 62 percent / Na2S2O4*H2O / ethanol / Heating
3: 1.) conc. aq. HCl, NaNO2 / 1.) H2O, 20 min, 2.) H2O, RT, 0.5 h
4: 37 percent / 40percent aq. HF / benzene / 1.) RT, 0.5 h, 2.) 50 deg C, 10 min
5: 1.) Mg / 2.) ether, 2.) ether, reflux, 4 h
6: 85 percent / BBr3 / CH2Cl2 / 1 h / Ambient temperature
7: KOH / ethanol / 20 h / Heating
View Scheme
参考文献
Shani; Gazit; Livshitz; Biran
Journal of Medicinal Chemistry, 1985 , vol. 28, # 10 p. 1504 - 1511
