1: pyrrole With methylmagnesium bromide in tetrahydrofuran; diethyl ether
T=-78 - 25°C; 1 h; Inert atmosphere;
2: 4-nitro-benzoyl chloride in tetrahydrofuran; diethyl ether
T=20°C; 3 h; Inert atmosphere;
参考文献
NATIONAL UNIVERSITY OF SINGAPORE; AGENCY FOR SCIENCE, TECHNOLOGY AND RESEARCH; CHANG, Young-Tae; LEE, Sung Chan; KANG, Nam-Young; YUN, Seong Wook; LEONG, Cheryl Kit Mun; HA, Hyung Ho
Patent: WO2013/95305 A1, 2013 ;
Location in patent: Page/Page column 25 ;
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane
T=23°C; 15 h;
参考文献
Ayala, Leticia; Lucero, Claudia G.; Antoinette, Jan; Romero; Tabacco, Sarah A.; Woerpel
Journal of the American Chemical Society, 2003 , vol. 125, # 50 p. 15521 - 15528
in benzene
reaction of ferrocenylcopper and p-nitrobenzoyl chloride in benzene for1.5 h under argon;
参考文献
Moiseev, S. K.; Sedova, N. N.; Sazonova, V. A.
Doklady Chemistry (English Translation), 1982 , vol. 267, p. 444 - 447
Doklady Akademii Nauk SSSR, 1982 , vol. 267, p. 1374 - 1378
