1,1,3,3-四乙氧基丙烷合成路线 （共 75 条）
反应条件
in ethanol; acetic acid 5 h; Heating;
参考文献
Kuenstlinger, M.; Breitmaier, E.
Synthesis, 1983 , # 2 p. 161 - 162
反应条件
ethanol; nitrogen T=200°C; Leiten ueber einen Montmorillonit-Katalysator;
参考文献
Bredereck et al.
Chemische Berichte, 1958 , vol. 91, p. 2832,2841
反应条件
ammonium acetate in xylene 16 h; Heating;
参考文献
Huang, Yanhe; Hartmann, Rolf W.
Synthetic Communications, 1998 , vol. 28, # 7 p. 1197 - 1200
反应条件
hydrogenchloride; triethylamine
参考文献
Protopopowa; Skoldinow
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 1276,1279; engl. Ausg. S. 1360, 1362
反应条件
1: 2-Nitrothiophene With hydrogenchloride; tin; zinc(II) chloride in ethanol T=85°C; 2: 1,1,3,3-tetraethoxy-propane in ethanol T=85°C; 1 h;
参考文献
SU, Wei-Guo; JIA, Hong; DAI, Guangxiu
Patent: US2012/245178 A1, 2012 ;
Location in patent: Page/Page column 19 ;
US 20120245178 A1
反应条件
ethanol; methyl hydrazine sulfate
参考文献
Finar; Lord
Journal of the Chemical Society, 1957 , p. 3314
反应条件
acetic acid 1.5 h; Heating;
参考文献
Kuenstlinger, M.; Breitmaier, E.
Synthesis, 1983 , # 1 p. 44 - 47
反应条件
in methanol HeatingReflux;
参考文献
UCHREZHDENIE ROSSIISKOI AKADEMII NAUK INSTITUT MOLEKULYARNOI BIOLOGII IM. V.A. ENGELGARDTA RAN (IMB RAN)
Patent: EP2157088 A1, 2010 ;
Location in patent: Page/Page column 55 ;
反应条件
phosphorus trichoride var. ratio of reagents, var. temp., var. time; Product distribution;
参考文献
Gazizov, M. B.; Gizatullina, I. Kh.; Razumov, A. I.; Ostanina, L. P.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 11 p. 2637 - 2638,2274
参考文献
Alley; Shirley
Journal of the American Chemical Society, 1958 , vol. 80, p. 6271,6273
