1,1,3,3-四乙氧基丙烷合成路线 (共 75 条)
反应条件
in hydrogenchloride; methanol T=50°C; 25 h;
参考文献
Pfaendler; Maier; Klar
Journal of the American Chemical Society, 1986 , vol. 108, # 6 p. 1338 - 1339
参考文献
Hunt et al.
Journal of the Chemical Society, 1959 , p. 525,528
Full Text Show Details
Protopopowa; Skoldinow
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 1276,1279; engl. Ausg. S. 1360, 1362
反应条件
(i) aq. TsOH, (ii) /BRN= 741982/; Multistep reaction;
参考文献
Kucera,J. et al.
Collection of Czechoslovak Chemical Communications, 1970 , vol. 35, p. 3618 - 3627
参考文献
Hunt et al.
Journal of the Chemical Society, 1959 , p. 525,528
Full Text Show Details
Crosby et al.
Org. Synth. Coll. Vol. V, <1973> 703
参考文献
Protopopowa; Skoldinow
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 1276,1279; engl. Ausg. S. 1360, 1362
参考文献
Journal of the Chemical Society, , p. 3024,3025
反应条件
hydrogenchloride in diethyl ether; dichloromethane
参考文献
Stavrovskaya,A.V. et al.
Journal of Organic Chemistry USSR (English Translation), 1971 , vol. 7, p. 260 - 265
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, p. 267 - 273
参考文献
Khasapov,B.N. et al.
Zhurnal Organicheskoi Khimii, 1973 , vol. 9, p. 20 - 23,17 - 20
反应条件
Bu4NBHCl3 in benzene T=65 - 70°C; 6 h;
参考文献
Kryshtal', G. V.; Gavrilova, L. A.; Titov, L. V.; Yanovskaya, L. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 5 p. 907 - 909
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 5 p. 1146 - 1148
反应条件
zinc(II) chloride 1.) ethyl acetate, 40 deg C, 0.25 hr., 2.) ethanol, 20 deg C, 4 hrs.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, p. 1281 - 1286
Zhurnal Organicheskoi Khimii, , vol. 21, # 7 p. 1408 - 1413