1.1: sulfur; iodine / 2 h / 170 °C
2.1: sodium hydride / N,N-dimethyl-formamide / 0 - 25 °C
2.2: 25 °C
3.1: sodium azide / dimethyl sulfoxide; water / 48 h / 25 °C
3.2: 50 °C
View Scheme
Kharasch; Kleiger; Mayo
Journal of Organic Chemistry, 1939 , vol. 4, p. 431,434
Full Text Show Details
Kharasch; Hannum
Journal of the American Chemical Society, 1934 , vol. 56, p. 712
Kharasch; Kleiger; Mayo
Journal of Organic Chemistry, 1939 , vol. 4, p. 431,434
Full Text Show Details
Kharasch; Hannum
Journal of the American Chemical Society, 1934 , vol. 56, p. 712
1: 2-bromo acetyl bromide With poly(ethylene glycol) 3400; N-ethyl-N,N-diisopropylamine in dichloromethane
T=20°C;
2: diphenylamine in dichloromethane
T=20°C;
3: With sodium hydroxide in water
T=60°C;
