反应条件
1: tri-n-butylborane; methylmagnesium bromide in tetrahydrofuran
T=0 - 25°C; 1.5 h; Inert atmosphere;
2: 7-bromo-heptanonitrile With N-undecane; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran
T=0°C; 1 h; Inert atmosphere;
3: With iron (III) acetylacetonate in tetrahydrofuran
T=0 - 25°C; 7 h; Inert atmosphere;
参考文献
Hatakeyama, Takuji; Hashimoto, Toru; Kathriarachchi, Kalum K. A. D. S.; Zenmyo, Takeshi; Seike, Hirofumi; Nakamura, Masaharu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 35 p. 8834 - 8837
