对乙氧基-N-乙酰乙酰苯胺合成路线 (共 8 条)
反应条件
triethylamine in benzene T=10°C; RefluxInert atmosphere;
参考文献
Osolodkin, Dmitry I.; Kozlovskaya, Liubov I.; Dueva, Evgenia V.; Dotsenko, Victor V.; Rogova, Yulia V.; Frolov, Konstantin A.; Krivokolysko, Sergey G.; Romanova, Ekaterina G.; Morozov, Alexey S.; Karganova, Galina G.; Palyulin, Vladimir A.; Pentkovski, Vladimir M.; Zefirov, Nikolay S.
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 9 p. 869 - 874
参考文献
Jones, Raymond C. F.; Collighan, Russell J.; Crane, Joanna; Hodges, Nikolas J.; Ling, Matthew S.; Stroud, Joanne
Synthetic Communications, 2002 , vol. 32, # 20 p. 3185 - 3191
参考文献
Chemische Berichte, , vol. 64, p. 969
反应条件
methanol; nickel Hydrogenation;
参考文献
Farbw. Hoechst
Patent: US2830087 , 1956 ;
反应条件
1: concentrated sulfuric acid / 100 °C
2: phosphoryl chloride
View Scheme
参考文献
Backeberg
Journal of the Chemical Society, 1933 , p. 1031
反应条件
[bis(acetoxy)iodo]benzene; zinc dibromide in 1,4-dioxane
T=20°C; 1 h;
参考文献
Liu, Wei-Bing; Chen, Cui; Zhang, Qing; Zhu, Zhi-Bo
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 344 - 348
反应条件
sulfuric acid
T=100°C;
参考文献
Backeberg
Journal of the Chemical Society, 1933 , p. 1031