triphenylphosphine on polymer; diethylazodicarboxylate in tetrahydrofuran
Mitsunobu reaction; 2 h; Title compound not separated from byproducts;
参考文献
Harned, Andrew M.; He, Helen Song; Toy, Patrick H.; Flynn, Daniel L.; Hanson, Paul R.
Journal of the American Chemical Society, 2005 , vol. 127, # 1 p. 52 - 53
sulfur trioxide in CD3NO2
T=0°C; 0.24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Koeberg-Telder, Ankie; Griendt, Freek van de; Cerfontain, Hans
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 358 - 362
sulfuric acid
T=25°C; 0.24 h; Title compound not separated from byproducts;
参考文献
Koeberg-Telder, Ankie; Griendt, Freek van de; Cerfontain, Hans
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 358 - 362
sulfuric acid
T=25°C; 504 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Koeberg-Telder, Ankie; Griendt, Freek van de; Cerfontain, Hans
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 358 - 362
sulfuric acid
T=25°C; 504 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Koeberg-Telder, Ankie; Griendt, Freek van de; Cerfontain, Hans
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 358 - 362
sulfur trioxide in CD3NO2
T=-10°C; 504 h; variation of time and temperature; Product distributionMechanism;
参考文献
Koeberg-Telder, Ankie; Griendt, Freek van de; Cerfontain, Hans
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 358 - 362
sulfuric acid
T=5°C; 480 h; variation of time, concentration of H2SO4 and temperature; MechanismProduct distribution;
参考文献
Koeberg-Telder, Ankie; Griendt, Freek van de; Cerfontain, Hans
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 358 - 362
