1,3-双(4-氯苯基)硫脲合成路线 (共 30 条)
反应条件
2-chloro-1-methyl-pyridinium iodide in dimethyl sulfoxide
T=40°C; 0.5 h;
参考文献
Takikawa, Yuji; Inoue, Noriyuki; Sato, Ryu; Takizawa, Saburo
Chemistry Letters, 1982 , p. 641 - 642
参考文献
Li; Wang; Luo
Synthetic Communications, 2001 , vol. 31, # 5 p. 781 - 785
反应条件
in pyridine; water
T=60°C; Condensation; 48 h;
参考文献
Blanco, Jose L. Jimenez; Barria, Claudio Saitz; Benito, Juan M.; Mellet, Carmen Ortiz; Fuentes, Jose; Santoyo-Gonzales, Francisco; Fernandez, Jose M. Garcia
Synthesis, 1999 , # 11 p. 1907 - 1914
反应条件
sodium sulfide; N-benzyl-N,N,N-triethylammonium chloride in water
8 h; Ambient temperature;
参考文献
Broda, Witold; Dehmlow, Eckehard V.
Liebigs Annalen der Chemie, 1983 , # 10 p. 1839 - 1843
反应条件
PEG-400 in water
0.0333333 h; microwave irradiation;
参考文献
Li, Zheng; Wang, Zhi-Yuan; Zhao, Yan-Long; Xing, Yu-Lin; Zhu, Wei
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 12 p. 2745 - 2750
反应条件
mercury(II) diacetate; triethylamine in 1,4-dioxane
T=20°C;
参考文献
Singh, Okram Mukherjee; Singh, Sarangthem Joychandra
Journal of Chemical Research, 2006 , # 8 p. 483 - 485
反应条件
sodium ethanolate in N,N-dimethyl-formamide
T=80°C; 0.25 h;
参考文献
Li, Na; Tu, Man-Su; Jiang, Bo; Wang, Xiang; Tu, Shu-Jiang
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1743 - 1746
反应条件
2: 4.0 g / Raney nickel / benzene / 2.5 h / Heating
3: Raney nickel / ethanol / 1 h / Heating
View Scheme
参考文献
Ali, M. Umar; Meshram, H. M.; Paranjpe, M. G.
Journal of the Indian Chemical Society, 1985 , vol. 62, # 9 p. 666 - 669
反应条件
1: Raney nickel / ethanol / 1 h / Heating
View Scheme
参考文献
Ali, M. Umar; Meshram, H. M.; Paranjpe, M. G.
Journal of the Indian Chemical Society, 1985 , vol. 62, # 9 p. 666 - 669
反应条件
1: 4.0 g / Raney nickel / benzene / 2.5 h / Heating
2: Raney nickel / ethanol / 1 h / Heating
View Scheme
参考文献
Ali, M. Umar; Meshram, H. M.; Paranjpe, M. G.
Journal of the Indian Chemical Society, 1985 , vol. 62, # 9 p. 666 - 669