N-(4-(4,4,5,5-四甲基-1,3,2-二噁硼烷-2-基)吡啶-2-基)乙酰胺合成路线 (共 2 条)
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in N,N-dimethyl-formamide T=80°C; 3.5 h; Inert atmosphere;
参考文献
US2013/165464 A1, ;
Paragraph 0835 ;
反应条件
1: 4-(N,N-dimethlyamino)pyridine / 3 h / 140 °C 2: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 3.5 h / 80 °C / |Inert atmosphere View Scheme