反应条件
sodium amalgam in tetrahydrofuran (Ar); dropwise addn. (15 min) of soln. of Re carbonyl to Na amalgam, stirring, ca 20°C, 1 h, filtering, addn. of soln. of Cr complex, stirring, ca 20°C, 3 h; evapn. of solvent in vac., chromy. (Al2O3 / benzene), evapn. of solvent in vac.;
参考文献
Kaganovich, V. S.; Rybinskaya, M. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, p. 1503 - 1506
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , p. 1644 - 1647