Alpha-甲基-N-苯基-1H-苯并三唑合成路线 （共 4 条）
反应条件
in diethyl ether T=-20 - 0°C;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1382598 A1, 2004 ;
Location in patent: Page 39; 78 ;
反应条件
in diethyl ether T=22°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Katritzky, Alan R.; Rachwal, Bogumila; Rachwal, Stanislaw
Journal of Organic Chemistry, 1995 , vol. 60, # 13 p. 3993 - 4001
反应条件
lithium diisopropyl amide 1.) THF, -78 deg C, 0.5 h, 2.) -78 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Katrizky, Alan R.; Oniciu, Daniela C.; Mancheno, Balbino; Barcolk, Richard A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 1 p. 113 - 119
反应条件
lithium diisopropyl amide 1.) THF, -78 deg C, 0.5 h, 2.) -78 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Katrizky, Alan R.; Oniciu, Daniela C.; Mancheno, Balbino; Barcolk, Richard A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 1 p. 113 - 119
