N-(4-甲基苯甲酰)-甘氨酸乙酯合成路线 （共 12 条）
反应条件
copper(l) iodide; calcium carbonate in water; acetonitrile T=40°C; 6 h;
参考文献
Yoo, Woo-Jin; Li, Chao-Jun
Journal of the American Chemical Society, 2006 , vol. 128, # 40 p. 13064 - 13065
反应条件
tert.-butylhydroperoxide; copper(l) iodide; silver(I) iodate; calcium carbonate in water; acetonitrile T=40°C; 6 h;
参考文献
Giguere-Bisson, Maxime; Yoo, Woo-Jin; Li, Chao-Jun
Organic Syntheses, 2012 , vol. 88, p. 14 - 21
反应条件
triethylamine in 1,4-dioxane 0.0166667 h; Ambient temperature;
参考文献
Theocharis, A.B.; Maroulis, A.J.; Hadjiantoniou-Maroulis, C.P.; Alexandrou, N.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 619 - 621
反应条件
potassium carbonate in water; toluene T=-5 - 5°C;
参考文献
Munakata; Tanaka; Toyoshima
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 7 p. 2045 - 2051
反应条件
1: SOCl2, DMF / toluene / 0.5 h / 60 - 70 °C 2: K2CO3 / H2O; toluene / -5 - 5 °C View Scheme
参考文献
Munakata; Tanaka; Toyoshima
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 7 p. 2045 - 2051
反应条件
1: 35 percent / lead tetra-acetate / CH2Cl2; acetic acid / 0.5 h / 0 °C 2: 95 percent / triethylamine / dioxane / 0.02 h / Ambient temperature View Scheme
参考文献
Theocharis, A.B.; Maroulis, A.J.; Hadjiantoniou-Maroulis, C.P.; Alexandrou, N.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 619 - 621
反应条件
1: methanol / Ambient temperature 2: 35 percent / lead tetra-acetate / CH2Cl2; acetic acid / 0.5 h / 0 °C 3: 95 percent / triethylamine / dioxane / 0.02 h / Ambient temperature View Scheme
参考文献
Theocharis, A.B.; Maroulis, A.J.; Hadjiantoniou-Maroulis, C.P.; Alexandrou, N.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 619 - 621
反应条件
1: Iron (III) nitrate nonahydrate; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical / acetonitrile / 2 h / 20 °C / |Inert atmosphere; |Green chemistry 2: tert.-butylhydroperoxide; calcium carbonate / water / 16 h / 60 °C / |Inert atmosphere; |Green chemistry View Scheme
参考文献
Ghosh, Subhash Chandra; Ngiam, Joyce S.Y.; Seayad, Abdul M.; Tuan, Dang Thanh; Johannes, Charles W.; Chen, Anqi
Tetrahedron Letters, 2013 , vol. 54, # 36 p. 4922 - 4925
参考文献
Klages; Haack
Chemische Berichte, 1903 , vol. 36, p. 1648
反应条件
1: benzene; diluted NaOH-solution 2: alcoholic hydrochloric acid View Scheme
参考文献
Klages; Haack
Chemische Berichte, 1903 , vol. 36, p. 1648
