1-苯基-4-己炔-3-酮合成路线 (共 3 条)
反应条件
Celite; pyridinium chlorochromate in dichloromethane T=20°C; Cooling with ice;
参考文献
Kiyotsuka, Yohei; Kobayashi, Yuichi
Journal of Organic Chemistry, 2009 , vol. 74, # 19 p. 7489 - 7495
反应条件
1: 1,2-dibromo-propane With lithium diisopropyl amide in tetrahydrofuran; hexane T=-78 - 0°C; 2: N-methoxy-N-methyl-3-phenyl-propionamide in tetrahydrofuran; hexane T=-78 - 20°C; 3: With hydrogenchloride in tetrahydrofuran; hexane; water T=0°C;
参考文献
Journal of the American Chemical Society, , vol. 132, # 26 p. 8862 - 8863
反应条件
Yield given. Multistep reaction;
参考文献
Judge; Phillips; Morris; Lovasz; Romines; Luke; Tulinsky; Tustin; Chrusciel; Dolak; Mizsak; Watt; Vander Velde; Strohbach; Gammill
Journal of the American Chemical Society, 1997 , vol. 119, # 15 p. 3627 - 3628