1: 1.) TFAA / 2.) CH2Cl2, room t., 90 h; addition at 0, 6 and 48 h 2: 70 percent / silver(II)oxide / dioxane / Ambient temperature 3: 65 percent / BCl3(7 mol equiv) / CH2Cl2 / 3 h / 0 °C / then to room t. 4: 74 percent / nitrobenzene / 2 h / 200 °C View Scheme
参考文献
Koning, Charles B.; Giles, Robin G.F.; Engelhardt, Lutz M.; White, Allan H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3209 - 3216
(NH4)2S2O8; silver nitrate in water; acetonitrile
18 h; Ambient temperature;
参考文献
Tanoue, Yasuhiro; Sakata, Kazunori; Hashimoto, Mamoru; Morishita, Shin-ichi; Hamada, Moritsugu
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 9 p. 2593 - 2595
(NH4)2S2O8; silver nitrate in water; acetonitrile
18 h; Ambient temperature;
参考文献
Tanoue, Yasuhiro; Sakata, Kazunori; Hashimoto, Mamoru; Morishita, Shin-ichi; Hamada, Moritsugu
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 9 p. 2593 - 2595
Multi-step reaction with 2 steps 1: 1.) TFAA / 2.) CH2Cl2, room t., 90 h; addition at 0, 6 and 48 h2: 70 percent / silver(II)oxide / dioxane / Ambient temperature
参考文献
Koning, Charles B.; Giles, Robin G.F.; Engelhardt, Lutz M.; White, Allan H. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3209 - 3216
Multi-step reaction with 3 steps 1: 1.) TFAA / 2.) CH2Cl2, room t., 90 h; addition at 0, 6 and 48 h2: 70 percent / silver(II)oxide / dioxane / Ambient temperature3: 65 percent / BCl3(7 mol equiv) / CH2Cl2 / 3 h / 0 °C / then to room t.
参考文献
Koning, Charles B.; Giles, Robin G.F.; Engelhardt, Lutz M.; White, Allan H. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3209 - 3216
