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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
122183-01-1
合成路线
（共 9 条）
122183-01-1
→
反应条件
123-54-6
乙酰丙酮
反应条件
1: conc. hydrochloric acid, CH3CN / Heating 2: 55 percent / benzene / 8 h / Heating 3: conc. hydrochloric acid, CH3CN / Heating 4: 90 percent / benzene / 8 h / Heating 5: conc. hydrochloric acid, CH3CN / Heating 6: 70 percent / benzene / 8 h / Heating 7: conc. hydrochloric acid, CH3CN / Heating View Scheme
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 38, p. 157 - 166
122183-01-1
→
反应条件
122182-95-0
+
123-54-6
乙酰丙酮
反应条件
hydrogenchloride; acetonitrile Heating;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 38, p. 157 - 166
122183-01-1
→
反应条件
122182-96-1
反应条件
Multi-step reaction with 2 steps 1: conc. hydrochloric acid, CH3CN / Heating2: 65 percent / benzene / 8 h / Heating
参考文献
Khandelwal, Bishan L.; Singh, Ajai K.; Bhandari, Narendra S. Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 157 - 166
122183-01-1
→
反应条件
122182-97-2
反应条件
Multi-step reaction with 4 steps 1: conc. hydrochloric acid, CH3CN / Heating2: 55 percent / benzene / 8 h / Heating3: conc. hydrochloric acid, CH3CN / Heating4: 45 percent / benzene / 8 h / Heating
参考文献
Khandelwal, Bishan L.; Singh, Ajai K.; Bhandari, Narendra S. Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 157 - 166
122183-01-1
→
反应条件
122182-98-3
反应条件
Multi-step reaction with 4 steps 1: conc. hydrochloric acid, CH3CN / Heating2: 55 percent / benzene / 8 h / Heating3: conc. hydrochloric acid, CH3CN / Heating4: 90 percent / benzene / 8 h / Heating
参考文献
Khandelwal, Bishan L.; Singh, Ajai K.; Bhandari, Narendra S. Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 157 - 166
122183-01-1
→
反应条件
122182-99-4
反应条件
Multi-step reaction with 2 steps 1: conc. hydrochloric acid, CH3CN / Heating2: 55 percent / benzene / 8 h / Heating
参考文献
Khandelwal, Bishan L.; Singh, Ajai K.; Bhandari, Narendra S. Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 157 - 166
122182-97-2
→
反应条件
122183-01-1
反应条件
Multi-step reaction with 8 steps 1: conc. hydrochloric acid, CH3CN / Heating2: 55 percent / benzene / 8 h / Heating3: conc. hydrochloric acid, CH3CN / Heating4: 90 percent / benzene / 8 h / Heating5: conc. hydrochloric acid, CH3CN / Heating6: 70 percent / benzene / 8 h / Heating7: conc. hydrochloric acid, CH3CN / Heating8: 30 percent / benzene / 8 h / Ambient temperature
参考文献
Khandelwal, Bishan L.; Singh, Ajai K.; Bhandari, Narendra S. Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 157 - 166
122182-98-3
→
反应条件
122183-01-1
反应条件
Multi-step reaction with 8 steps 1: conc. hydrochloric acid, CH3CN / Heating2: 55 percent / benzene / 8 h / Heating3: conc. hydrochloric acid, CH3CN / Heating4: 45 percent / benzene / 8 h / Heating5: conc. hydrochloric acid, CH3CN / Heating6: 70 percent / benzene / 8 h / Heating7: conc. hydrochloric acid, CH3CN / Heating8: 30 percent / benzene / 8 h / Ambient temperature
参考文献
Khandelwal, Bishan L.; Singh, Ajai K.; Bhandari, Narendra S. Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 157 - 166
122182-99-4
→
反应条件
122183-01-1
反应条件
Multi-step reaction with 8 steps 1: conc. hydrochloric acid, CH3CN / Heating2: 90 percent / benzene / 8 h / Heating3: conc. hydrochloric acid, CH3CN / Heating4: 45 percent / benzene / 8 h / Heating5: conc. hydrochloric acid, CH3CN / Heating6: 70 percent / benzene / 8 h / Heating7: conc. hydrochloric acid, CH3CN / Heating8: 30 percent / benzene / 8 h / Ambient temperature
参考文献
Khandelwal, Bishan L.; Singh, Ajai K.; Bhandari, Narendra S. Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 157 - 166
