甲基4-亚氨基甲酰胺基苯甲酸酯合成路线 （共 4 条）
反应条件
thionyl chloride in methanol; dichloromethane
参考文献
Satoh, Yoshitaka; Bhagwat, Shripad S.
Patent: US2004/106634 A1, 2004 ;
US 20040106634 A1
反应条件
1: With acetyl chloride T=0 - 20°C; 16.33 h; Inert atmosphere; 2: With sodium hydrogencarbonate in methanol T=0°C;
参考文献
Melvin, JR., Lawrence S.; Graupe, Michael; Venkataramani, Chandrasekar
Patent: US2010/29638 A1, 2010 ;
Location in patent: Page/Page column 62 ;
US 20100029638 A1
反应条件
water; scandium tris(trifluoromethanesulfonate) T=20 - 100°C; 48 h; Overall yield = 63 percent;
参考文献
Tsubokura, Kazuki; Iwata, Takayuki; Taichi, Misako; Kurbangalieva, Almira; Fukase, Koichi; Nakao, Yoichi; Tanaka, Katsunori
Synlett, 2014 , vol. 25, # 9 p. 1302 - 1306
反应条件
potassium phosphate; copper(l) iodide; N-methyl-glycine in acetonitrile T=70°C; Ullmann reaction; 10 h; Inert atmosphere;
参考文献
Xing, Hui; Zhang, Ye; Lai, Yisheng; Jiang, Yongwen; Ma, Dawei
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5449 - 5453
