(4-甲氧基-3-甲基苯基)乙醛合成路线 （共 5 条）
反应条件
1: 65 percent / NaOCH3 / methanol / 1) -5 deg C, 2 h, 2) room temperature, 3 h 2: 1) NaOCH3, H2O, 2) AcOH / 1) MeOH, overnight, 2) benzene, H2O, 80 deg C View Scheme
参考文献
Cannon; True; Long; Bhatnagar; Leonard; Flynn
Journal of Medicinal Chemistry, 1989 , vol. 32, # 9 p. 2210 - 2214
反应条件
water; sodium methylate; acetic acid 1) MeOH, overnight, 2) benzene, H2O, 80 deg C; Yield given. Multistep reaction;
参考文献
Cannon; True; Long; Bhatnagar; Leonard; Flynn
Journal of Medicinal Chemistry, 1989 , vol. 32, # 9 p. 2210 - 2214
反应条件
ozone T=-20°C; und anschliessendes Erhitzen mit Wasser;
参考文献
Mumm; Diederichsen
Chemische Berichte, 1939 , vol. 72, p. 1523,1526
参考文献
Mumm; Diederichsen
Chemische Berichte, 1939 , vol. 72, p. 1523,1526
反应条件
1: 97 percent / benzene / 2 h / Heating
2: 99 percent / H2 / 5percent Pd-C / acetic acid / 2844.3 Torr / Ambient temperature
View Scheme
参考文献
Cannon; True; Long; Bhatnagar; Leonard; Flynn
Journal of Medicinal Chemistry, 1989 , vol. 32, # 9 p. 2210 - 2214
