in dichloromethane (N2); exclude moisture; added dropwise a soln. of B-compound to soln. of S-compound at -78°C under stirring; stirred for 12 h at -78°C; warmed to room temp.; distd. (vac.); elem. anal.;
参考文献
Habben, Carl D.; Heine, Andreas; Sheldrick, George M.; Stalke, Dietmar; Buehl, Michael; et al.
Chemische Berichte, 1991 , vol. 124, p. 47 - 50
in tetrachloromethane addn. of soln. of (t-BuN)2S to soln. of (t-BuN)2(BMe)2S2 (dropwise), treatment (18 h); sepn. of solvent, distn. (vac.); elem. anal.;
参考文献
Habben, Carl; Meller, Anton; Pusch, Stefan
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1988 , vol. 43, # 8 p. 959 - 962
