4-(二乙基氨基甲酰)苯甲酸甲酯合成路线 （共 4 条）
反应条件
Schwartz's reagent in tetrahydrofuran T=20°C; 0.416667 h; Inert atmosphere;
参考文献
Zhao, Yigang; Snieckus, Victor
Organic Letters, 2014 , vol. 16, # 2 p. 390 - 393
反应条件
anhydrous sodium hydrogen carbonate; sodium chloride in dichloromethane; N,N-dimethyl-formamide
参考文献
Toyama Chemical Co., Ltd.
Patent: US6384065 B1, 2002 ;
反应条件
in dichloromethane
T=20°C; 0.5 h; Cooling with ice;
参考文献
Leighty, Matthew W.; Spletstoser, Jared T.; Georg, Gunda I.
Organic Syntheses, 2012 , vol. 88, p. 427 - 437
反应条件
1: thionyl chloride; N,N-dimethyl-formamide / toluene / 20 °C
2: triethylamine / dichloromethane / 0 - 20 °C
View Scheme
参考文献
Zhao, Yigang; Snieckus, Victor
Organic Letters, 2014 , vol. 16, # 2 p. 390 - 393
