N-叔丁氧羰基-1,5-亚氨基-D-山梨糖醇合成路线 （共 7 条）
反应条件
10 palladium on activated carbon; hydrogen in methanol; ethyl acetate
参考文献
Heuckendorff, Mads; Pedersen, Christian M.; Bols, Mikael
Chemistry - A European Journal, 2010 , vol. 16, # 47 p. 13982 - 13994
反应条件
in N,N-dimethyl-formamide T=20°C; 15 h;
参考文献
Danieli, Elisa; Lalot, Jerome; Murphy, Paul V.
Tetrahedron, 2007 , vol. 63, # 29 p. 6827 - 6834
反应条件
1: 92 percent / H2O; Dowex-50-X8-100 (H(1+)) / acetonitrile / 3 h / Heating 2: H2 / Pd(OH)2/C / methanol / 12 h / 20 °C / 760.05 Torr 3: 1.28 g / H2; HCl / Pd(OH)2/C / methanol / 2 h / 20 °C / 760.05 Torr 4: 61 percent / dimethylformamide / 15 h / 20 °C View Scheme
参考文献
Danieli, Elisa; Lalot, Jerome; Murphy, Paul V.
Tetrahedron, 2007 , vol. 63, # 29 p. 6827 - 6834
反应条件
1: H2 / Pd(OH)2/C / methanol / 12 h / 20 °C / 760.05 Torr 2: 1.28 g / H2; HCl / Pd(OH)2/C / methanol / 2 h / 20 °C / 760.05 Torr 3: 61 percent / dimethylformamide / 15 h / 20 °C View Scheme
参考文献
Danieli, Elisa; Lalot, Jerome; Murphy, Paul V.
Tetrahedron, 2007 , vol. 63, # 29 p. 6827 - 6834
反应条件
1: 73 percent / NaH / dimethylformamide / 2 h / 0 °C 2: 85 percent / aq. AcOH / 2 h / 60 °C 3: SOCl2; pyridine / tetrahydrofuran / 2 h / 0 °C 4: 15 g / NaN3 / dimethylformamide / 16 h / 110 °C 5: 92 percent / H2O; Dowex-50-X8-100 (H(1+)) / acetonitrile / 3 h / Heating 6: H2 / Pd(OH)2/C / methanol / 12 h / 20 °C / 760.05 Torr 7: 1.28 g / H2; HCl / Pd(OH)2/C / methanol / 2 h / 20 °C / 760.05 Torr 8: 61 percent / dimethylformamide / 15 h / 20 °C View Scheme
参考文献
Danieli, Elisa; Lalot, Jerome; Murphy, Paul V.
Tetrahedron, 2007 , vol. 63, # 29 p. 6827 - 6834
反应条件
1: 85 percent / aq. AcOH / 2 h / 60 °C 2: SOCl2; pyridine / tetrahydrofuran / 2 h / 0 °C 3: 15 g / NaN3 / dimethylformamide / 16 h / 110 °C 4: 92 percent / H2O; Dowex-50-X8-100 (H(1+)) / acetonitrile / 3 h / Heating 5: H2 / Pd(OH)2/C / methanol / 12 h / 20 °C / 760.05 Torr 6: 1.28 g / H2; HCl / Pd(OH)2/C / methanol / 2 h / 20 °C / 760.05 Torr 7: 61 percent / dimethylformamide / 15 h / 20 °C View Scheme
参考文献
Danieli, Elisa; Lalot, Jerome; Murphy, Paul V.
Tetrahedron, 2007 , vol. 63, # 29 p. 6827 - 6834
反应条件
1: SOCl2; pyridine / tetrahydrofuran / 2 h / 0 °C 2: 15 g / NaN3 / dimethylformamide / 16 h / 110 °C 3: 92 percent / H2O; Dowex-50-X8-100 (H(1+)) / acetonitrile / 3 h / Heating 4: H2 / Pd(OH)2/C / methanol / 12 h / 20 °C / 760.05 Torr 5: 1.28 g / H2; HCl / Pd(OH)2/C / methanol / 2 h / 20 °C / 760.05 Torr 6: 61 percent / dimethylformamide / 15 h / 20 °C View Scheme
参考文献
Danieli, Elisa; Lalot, Jerome; Murphy, Paul V.
Tetrahedron, 2007 , vol. 63, # 29 p. 6827 - 6834
