反应条件
Multi-step reaction with 3 steps 1: oxalyl chloride, DMF / CH2Cl2 / 18 h / Ambient temperature2: 1.) n-BuLi, 2,2'-bipyridyl / 1.) THF, hexane, from -20 deg C to -5 deg C, 2.) THF, hexane, -30 deg C, 2 h3: acetic anhydride / 22 h / Heating
参考文献
Sanchez, Joseph P.; Gogliotti, Rocco D.; Domagala, John M.; Gracheck, Stephen J.; Huband, Michael D.; et al. Journal of Medicinal Chemistry, 1995 , vol. 38, # 22 p. 4478 - 4487
