三丁基(3-甲氧基苯基)锡合成路线 （共 12 条）
反应条件
trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile CoBr2 and Zn dust activated with CF3CO2H reacted for 5 min with allyl chloride in MeCN, aryl halide and tributylstannyl chloride added simultaneously in MeCN at room temp., stirred for 1.5 h at 50°C;
参考文献
Gosmini, Corinne; Perichon, Jacques
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 2 p. 216 - 217
反应条件
magnesium; ethylene dibromide in tetrahydrofuran T=35°C; Barbier Coupling Reaction; 1 h; SonicationInert atmosphere; regioselective reaction;
参考文献
Gerbino, Dario C.; Fidelibus, Pablo M.; Mandolesi, Sandra D.; Ocampo, Romina A.; Scoccia, Jimena; Podesta, Julio C.
Journal of Organometallic Chemistry, 2013 , vol. 741-742, # 1 p. 24 - 32
反应条件
aluminium trichloride in dichloromethane T=-78°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Niestroj, Michael; Neumann, Wilhelm P.
Chemische Berichte, 1996 , vol. 129, # 1 p. 45 - 51
反应条件
bis-triphenylphosphine-palladium(II) chloride in toluene T=90°C; Stille Cross Coupling; 0.5 h; Inert atmosphere;
参考文献
Luong, Martin; Domini, Claudia E.; Silbestri, Gustavo F.; Chopa, Alicia B.
Journal of Organometallic Chemistry, 2013 , vol. 723, p. 43 - 48
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; Stille coupling; 0.5 h; Sonication;
参考文献
Ultrasonics Sonochemistry, , vol. 19, # 3 p. 410 - 414
反应条件
potassium peroxymonosulfate; potassium chloride; acetic acid in tetrahydrofuran T=95°C; 0.166667 h; SolventTemperatureTime; regioselective reaction;
参考文献
Takada, Yuuki; Hanyu, Masayuki; Nagatsu, Kotaro; Fukumura, Toshimitsu
Journal of Labelled Compounds and Radiopharmaceuticals, 2012 , vol. 55, # 10 p. 383 - 386,4
反应条件
bis-triphenylphosphine-palladium(II) chloride in toluene T=90°C; Stille Cross Coupling; 0.5 h; Inert atmosphere;
参考文献
Luong, Martin; Domini, Claudia E.; Silbestri, Gustavo F.; Chopa, Alicia B.
Journal of Organometallic Chemistry, 2013 , vol. 723, p. 43 - 48
反应条件
bis-triphenylphosphine-palladium(II) chloride in toluene T=90°C; Stille Cross Coupling; 0.5 h; Inert atmosphereSonication;
参考文献
Luong, Martin; Domini, Claudia E.; Silbestri, Gustavo F.; Chopa, Alicia B.
Journal of Organometallic Chemistry, 2013 , vol. 723, p. 43 - 48
反应条件
sulfuryl dichloride T=20°C; 4 h;
参考文献
Lube, Andreas; Neumann, Wilhelm P.; Niestroj, Michael
Chemische Berichte, 1995 , vol. 128, # 12 p. 1195 - 1198
反应条件
tetrakis(triphenylphosphine) palladium(0); 1-chloro-3-methyl-5,5-dimethoxy-(2E/Z)-pentene in N,N-dimethyl-formamide T=100°C; Yields of byproduct given;
参考文献
Ono, Machiko; Yoshida, Norio; Akita, Hiroyuki
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 11 p. 1745 - 1750
