1,3-二(4-甲氧苯基)-1,1,3,3-四甲基二硅氧烷合成路线 （共 21 条）
反应条件
n-butyllithium 1.) hexane, THF, Et2O, n-pentane, -110 deg C, 2 h, 2.) hexane, THF, Et2O, n-pentane, a) -110 deg C, 30 min, b) -110 deg C - RT, overnight; Multistep reaction. Title compound not separated from byproducts;
参考文献
Eaborn, Colin; Jones, Karen L.; Lickiss, Paul D.
Journal of Organometallic Chemistry, 1994 , vol. 466, # 1-2 p. 35 - 42
反应条件
9,10-anthracenedicarbonitrile; oxygen; H218O in acetonitrile 0.75 h; Ambient temperatureIrradiationvarious concentrations of H2(18)O; Product distribution;
参考文献
Mizuno, Kazuhiko; Tamai, Toshiyuki; Hashida, Isao; Otsuji, Yoshio
Journal of Organic Chemistry, 1995 , vol. 60, # 9 p. 2935 - 2937
反应条件
1.) hexane, THF, Et2O, n-pentane, -110 deg C, 2 h, 2.) hexane, THF, Et2O, n-pentane, a) -110 deg C, 30 min, b) -110 deg C - RT, overnight; Multistep reaction. Title compound not separated from byproducts;
参考文献
Eaborn, Colin; Jones, Karen L.; Lickiss, Paul D.
Journal of Organometallic Chemistry, 1994 , vol. 466, # 1-2 p. 35 - 42
反应条件
bis(η3-allyl-μ-chloropalladium(II)); 1,4-di(diphenylphosphino)-butane; potassium hydroxide in water; tert-butyl alcohol T=90°C; 16 h;
参考文献
Boehner, Christine M.; Frye, Elizabeth C.; O'Connell, Kieron M. G.; Galloway, Warren R. J. D.; Sore, Hannah F.; Dominguez, Patricia Garcia; Norton, David; Hulcoop, David G.; Owen, Martin; Turner, Gillian; Crawford, Claire; Horsley, Helen; Spring, David R.
Chemistry - A European Journal, 2011 , vol. 17, # 47 p. 13230 - 13239
反应条件
bis(η3-allyl-μ-chloropalladium(II)); tri-tert-butyl phosphine; potassium hydroxide in water; toluene; tert-butyl alcohol T=80°C;
参考文献
Chemistry - A European Journal, , vol. 17, # 47 p. 13230 - 13239
反应条件
bis(η3-allyl-μ-chloropalladium(II)); tri-tert-butyl phosphine; potassium hydroxide in water; toluene; tert-butyl alcohol T=80°C;
参考文献
Boehner, Christine M.; Frye, Elizabeth C.; O'Connell, Kieron M. G.; Galloway, Warren R. J. D.; Sore, Hannah F.; Dominguez, Patricia Garcia; Norton, David; Hulcoop, David G.; Owen, Martin; Turner, Gillian; Crawford, Claire; Horsley, Helen; Spring, David R.
Chemistry - A European Journal, 2011 , vol. 17, # 47 p. 13230 - 13239
反应条件
hydrogenchloride in 1,4-dioxane; benzene T=29.9°C; without added water; Rate constant;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 141 - 150
反应条件
bis(η3-allyl-μ-chloropalladium(II)); tri-tert-butyl phosphine; potassium hydroxide in water; toluene; tert-butyl alcohol
T=80°C;
参考文献
Boehner, Christine M.; Frye, Elizabeth C.; O'Connell, Kieron M. G.; Galloway, Warren R. J. D.; Sore, Hannah F.; Dominguez, Patricia Garcia; Norton, David; Hulcoop, David G.; Owen, Martin; Turner, Gillian; Crawford, Claire; Horsley, Helen; Spring, David R.
Chemistry - A European Journal, 2011 , vol. 17, # 47 p. 13230 - 13239
反应条件
tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; silver(l) oxide in tetrahydrofuran
T=70°C; Hiyama-type coupling; 18 h;
参考文献
Napier, Spencer; Marcuccio, Sebastian M.; Tye, Heather; Whittaker, Mark
Tetrahedron Letters, 2008 , vol. 49, # 24 p. 3939 - 3942
反应条件
bis(η3-allyl-μ-chloropalladium(II)); 1,4-di(diphenylphosphino)-butane; potassium hydroxide in water; tert-butyl alcohol
T=90°C; 16 h;
参考文献
Boehner, Christine M.; Frye, Elizabeth C.; O'Connell, Kieron M. G.; Galloway, Warren R. J. D.; Sore, Hannah F.; Dominguez, Patricia Garcia; Norton, David; Hulcoop, David G.; Owen, Martin; Turner, Gillian; Crawford, Claire; Horsley, Helen; Spring, David R.
Chemistry - A European Journal, 2011 , vol. 17, # 47 p. 13230 - 13239
