1,3-二(2-甲氧基苯基)脲合成路线 （共 27 条）
反应条件
1,10-phenanthroline; Pd(1,10-phenanthroline)2(OTf)2
T=135°C; P=45003.6 Torr; 2 h; Further byproducts given;
参考文献
Wchman, Petra; Borst, Leo; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
Chemische Berichte, 1997 , vol. 130, # 1 p. 13 - 21
参考文献
Dains; Wertheim
Journal of the American Chemical Society, 1920 , vol. 42, p. 2308
反应条件
in benzene
Ambient temperature; Yield given;
参考文献
Etter, Margaret C.; Urbanczyk-Lipkowska, Zofia; Zia-Ebrahimi, Mohammad; Panunto, Thomas W.
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8415 - 8426
反应条件
1: 85 percent / phosphorus trichloride / 0.5 h / 110 °C
2: 91 percent / NaOH / dimethylsulfoxide / 0.5 h / 80 °C
View Scheme
参考文献
Atanassova, Ivanka A.; Petrov, Jan S.; Mollov, Nikola M.
Synthesis, 1987 , # 8 p. 734 - 736
反应条件
sodium azide; Pd2(dba)5; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran; hexane; water
T=50°C; 7 h;
参考文献
Miloserdov, Fedor M.; Grushin, Vladimir V.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 15 p. 3668 - 3672
参考文献
Curtet, Sophie; Langlois, Michel
Tetrahedron Letters, 1999 , vol. 40, # 49 p. 8563 - 8566
反应条件
in acetone
T=25°C; 60 h;
参考文献
Cotarca, Livius; Bacaloglu, R.; Csunderlik, C.; Marcu, N.; Tarnaveanu, A.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 6 p. 1052 - 1062
参考文献
Foerster
Chemische Berichte, 1888 , vol. 21, p. 1870
反应条件
in tetrahydrofuran
5 h; Photolysis;
参考文献
Cui, Yanyan; Spann, Andrew P.; Couch, Letha H.; Gopee, Neera V.; Evans, Frederick E.; Churchwell, Mona I.; Williams, Lee D.; Doerge, Daniel R.; Howard, Paul C.
Photochemistry and Photobiology, 2004 , vol. 80, # 2 p. 175 - 184
反应条件
1: tin; hydrochloric acid
2: benzene
View Scheme
参考文献
Muehlhaeuser
Justus Liebigs Annalen der Chemie, 1881 , vol. 207, p. 247
