4-叠氮基-2,3,5,6-四氟苯甲酰胺合成路线 （共 6 条）
反应条件
sodium azide in water; acetone 8 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 55, # 11 p. 3640 - 3647
反应条件
sodium hydroxide; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane T=25°C; 40 h;
参考文献
Journal of Organic Chemistry, , vol. 55, # 11 p. 3640 - 3647
反应条件
1: 49 percent / NH3 / dimethylsulfoxide / 120 h / 75 °C 2: 88 percent / Amberlyst 15 / 70 h / Heating 3: 98 percent / 20percent aq. NaOH / H2O; methanol View Scheme
参考文献
Keana, John F. W.; Cai, Sui Xiong
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3640 - 3647
反应条件
sodium peroxide in water T=50°C; 42 h;
参考文献
Keana, John F. W.; Cai, Sui Xiong
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3640 - 3647
反应条件
1: 64 percent / Na2O2 / H2O / 42 h / 50 °C 2: 99 percent / dicyclohexylcarbodiimide / CH2Cl2 / 25 °C View Scheme
参考文献
Keana, John F. W.; Cai, Sui Xiong
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3640 - 3647
反应条件
1: 64 percent / Na2O2 / H2O / 42 h / 50 °C 2: 70 percent / SOCl2 / CH2Cl2 / 36 h / Heating View Scheme
参考文献
Keana, John F. W.; Cai, Sui Xiong
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3640 - 3647
