反应条件
in toluene refluxing a mixt. of Rh-complex and Pt-compd. in toluene for 2 h (under N2, Schlenk technique);; pumping off, extn. (CH2Cl2), filtn. yields Pt-compd., evapn. of extract, chromy., elution (CH2Cl2/hexane) yields Rh-complex, elution (CH2Cl2), evapn., slow addn. of Et2O, cooling (-15°C), filtn., washing (Et2O), drying in vac., elem. anal.;;
参考文献
Ciriano, Miguel A.; Perez-Torrente, Jesus J.; Lahoz, Fernando J.; Oro, Luis A.
Inorganic Chemistry, 1992 , vol. 31, p. 969 - 974
